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            <gco:CharacterString>Cite this dataset as: Leinen, M. (2002) Calcium carbonate concentrations from sediment cores collected during R/V Thomas G. Thompson cruise TT013 in the Equatorial Pacific in 1992 during the U.S. JGOFS Equatorial Pacific (EqPac) project. Biological and Chemical Oceanography Data Management Office (BCO-DMO). (Version August 01, 2002) Version Date 2002-08-01 [if applicable, indicate subset used]. http://lod.bco-dmo.org/id/dataset/2703 [access date]</gco:CharacterString>
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        <gco:CharacterString>Calcium Carbonate concentrations, sediment cores Dataset Description: &amp;lt;p&amp;gt;Calcium Carbonate concentrations, sediment cores&amp;lt;/p&amp;gt; Methods and Sampling: &amp;lt;pre&amp;gt;
   &amp;lt;b&amp;gt;PI:&amp;lt;/b&amp;gt;              Margaret Leinen
   &amp;lt;b&amp;gt;of:&amp;lt;/b&amp;gt;              University of Rhode Island, Grad. School of Oceanography
   &amp;lt;b&amp;gt;dataset:&amp;lt;/b&amp;gt;         Calcium Carbonate concentrations, sediment cores
   &amp;lt;b&amp;gt;dates:&amp;lt;/b&amp;gt;           November 07, 1992 to November 29, 1992
   &amp;lt;b&amp;gt;location:&amp;lt;/b&amp;gt;        N: 4.0433  S: -4.9605  W: -140.1467  E: -139.4015
   &amp;lt;b&amp;gt;project/cruise:&amp;lt;/b&amp;gt;  EqPac/TT013 - Benthic survey
   &amp;lt;b&amp;gt;ship:&amp;lt;/b&amp;gt;            R/V Thomas Thompson

&amp;lt;/pre&amp;gt;
&amp;lt;!-- &amp;lt;b&amp;gt;&amp;lt;a href=&amp;quot;http://usjgofs.whoi.edu/PI-NOTES/eqpac/eqpac13_leinen.html&amp;quot;&amp;gt;Methodology&amp;lt;/a&amp;gt;&amp;lt;/b&amp;gt; --&amp;gt;
&amp;lt;p&amp;gt;&amp;lt;b&amp;gt;Carbonate analysis methodology:&amp;lt;/b&amp;gt;     Calcium carbonate was determined from inorganic carbon measurements made  on a Coulometrics Inc. Model 5011 CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; coulometer with a Model 5030 carbonate  carbon apparatus.  Between 5 and 10 mg of sample were acidified with 2ml 2N HCl to evolve CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;.  The CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; gas was bubbled into a titration cell where CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; was converted to hydroxyethylcarbonic acid which was automatically titrated  with a coulometrically-generated base to a colorimetric endpoint.  Grams of  carbon in the sample are calculated based on factory standardization of the  coulometric titration.  Calcium carbonate content was calculated by assuming  that all inorganic carbon in the sample was present as calcium carbonate, a  reasonable assumption for these biogenic sediments which contain little or  no dolomite.  The CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; coulometer has an accuracy of 0.15 &amp;amp;micro;g carbon.  The  precision of the complete procedure is &amp;amp;plusmn;0.52 wt% calcium carbonate based on  the standard deviation of a lab standard of deep sea sediment which we  developed from the study area.  Duplicate analyses were performed on every  tenth sample and an additional analysis was made for every pair which  differed by more than 2 wt%.&amp;lt;/p&amp;gt;
&amp;lt;p&amp;gt;&amp;amp;nbsp;&amp;lt;/p&amp;gt;</gco:CharacterString>
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   &amp;lt;b&amp;gt;location:&amp;lt;/b&amp;gt;        N: 4.0433  S: -4.9605  W: -140.1467  E: -139.4015
   &amp;lt;b&amp;gt;project/cruise:&amp;lt;/b&amp;gt;  EqPac/TT013 - Benthic survey
   &amp;lt;b&amp;gt;ship:&amp;lt;/b&amp;gt;            R/V Thomas Thompson

&amp;lt;/pre&amp;gt;
&amp;lt;!-- &amp;lt;b&amp;gt;&amp;lt;a href=&amp;quot;http://usjgofs.whoi.edu/PI-NOTES/eqpac/eqpac13_leinen.html&amp;quot;&amp;gt;Methodology&amp;lt;/a&amp;gt;&amp;lt;/b&amp;gt; --&amp;gt;
&amp;lt;p&amp;gt;&amp;lt;b&amp;gt;Carbonate analysis methodology:&amp;lt;/b&amp;gt;     Calcium carbonate was determined from inorganic carbon measurements made  on a Coulometrics Inc. Model 5011 CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; coulometer with a Model 5030 carbonate  carbon apparatus.  Between 5 and 10 mg of sample were acidified with 2ml 2N HCl to evolve CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;.  The CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; gas was bubbled into a titration cell where CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; was converted to hydroxyethylcarbonic acid which was automatically titrated  with a coulometrically-generated base to a colorimetric endpoint.  Grams of  carbon in the sample are calculated based on factory standardization of the  coulometric titration.  Calcium carbonate content was calculated by assuming  that all inorganic carbon in the sample was present as calcium carbonate, a  reasonable assumption for these biogenic sediments which contain little or  no dolomite.  The CO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; coulometer has an accuracy of 0.15 &amp;amp;micro;g carbon.  The  precision of the complete procedure is &amp;amp;plusmn;0.52 wt% calcium carbonate based on  the standard deviation of a lab standard of deep sea sediment which we  developed from the study area.  Duplicate analyses were performed on every  tenth sample and an additional analysis was made for every pair which  differed by more than 2 wt%.&amp;lt;/p&amp;gt;
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