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            <gco:CharacterString>Cite this dataset as: Church, M. J., White, A. E., Goetze, E., Ferron, S., Maloney, A. (2021) Particulate phosphate, particulate carbon, particulate nitrogen, particulate bulk isotope composition (C and N), and dissolved oxygen from Niskin bottle samples collected on R/V Kilo Moana cruise KM1910 in June 2019. Biological and Chemical Oceanography Data Management Office (BCO-DMO). (Version 1) Version Date 2021-05-20 [if applicable, indicate subset used]. doi:10.26008/1912/bco-dmo.852179.1 [access date]</gco:CharacterString>
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        <gco:CharacterString>Niskin bottle samples Dataset Description: &amp;lt;p&amp;gt;Particulate phosphate, particulate carbon, particulate nitrogen, particulate bulk isotope composition (C and N), and dissolved oxygen, collected with Niskin bottles during CTD deployments in June 2019 at station ALOHA during cruise KM1910.&amp;lt;/p&amp;gt; Methods and Sampling: &amp;lt;p&amp;gt;CTD and Niskin sampling follow HOT procedures summarized in detail: &amp;lt;a href=&amp;quot;https://hahana.soest.hawaii.edu/hot/protocols/protocols.html#&amp;quot; target=&amp;quot;_blank&amp;quot;&amp;gt;https://hahana.soest.hawaii.edu/hot/protocols/protocols.html#&amp;lt;/a&amp;gt;&amp;lt;/p&amp;gt;

&amp;lt;p&amp;gt;Dissolved Oxygen sampling and titrations from Niskin bottles follow HOT procedures. Briefly, oxygen samples were the first samples drawn from the Niskin bottles as soon as the rosette arrived on deck, free of bubbles, and fixed. Samples were analyzed with a computer controlled potentiometric titration. At 2 depths on each cast, 3 titrations were performed and had an average standard deviation of 0.4 micromol/L.&amp;lt;/p&amp;gt;

&amp;lt;p&amp;gt;Particulate Carbon and Nitrogen field and laboratory protocols follow HOT procedures (except sample analysis took place at Princeton University using a Vario ISOTOPE select EA-IRMS). Briefly, 4 to 20 L of water was collected from Niskin bottles, pre-filtered with an inline 202um mesh screen, and collected on combusted 25mm GF/F (Whatman, nominal pore size 0.7um), folded, and wrapped in clean (combusted) foil for storage at -20 degrees C until laboratory analysis. Samples were oven dried at 55-60 degrees celsius (samples were not acidified so C represents total C), pelletized in 9x11 tins, and analyzed via EA-IRMS for particulate carbon, delta-13C particulate carbon, particulate nitrogen, delta-15N particulate nitrogen. Six blank (dry) filters were analyzed for background C and N and subtracted from measured PC and PN sample values.&amp;lt;/p&amp;gt;

&amp;lt;p&amp;gt;Particulate Phosphate field and laboratory protocols follow HOT procedures. Briefly, 4 to 10 L of water was collected from Niskin bottles, pre-filtered with an inline 202um mesh screen, and collected on combusted 25mm GF/F (Whatman, nominal pore size 0.7um), folded, and placed in clean glass tube, storage at -20 degrees C until laboratory analysis. One sample from each depth was combusted in 16 x 100 mm clean glass test tubes at 450°C for 4.5 hours in a muffle furnace, allowed to cool and immersed in 10ml 0.15N HCL/vortex/ 1 hour leach/vortex/30 Minute Spin/ 1 hour color development) (5ml sample : 500ul Mixed Reagent). The liberated orthophosphate is reacted with a mixed reagent of molybdic acid, ascorbic acid and trivalent antimony to form phosphomolybdic acid. This heteropoly acid is then reduced to the colored molybdenum blue complex by ascorbic acid and the solution is measured spectrophotometrically. This procedure measures all forms of phosphorus which can be released by combustion and acid hydrolysis. Three blank (dry) filters were analyzed for background P and subtracted from measured PP sample values.&amp;lt;/p&amp;gt;</gco:CharacterString>
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        <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/award/805875.rdf" xlink:title="OCE-1911831" xlink:actuate="onRequest">Funding provided by NSF Division of Ocean Sciences (NSF OCE) Award Number: OCE-1911831 Award URL: https://www.nsf.gov/awardsearch/show-award?AWD_ID=1911831</gmx:Anchor>
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        <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/award/805880.rdf" xlink:title="OCE-1911990" xlink:actuate="onRequest">Funding provided by NSF Division of Ocean Sciences (NSF OCE) Award Number: OCE-1911990 Award URL: https://www.nsf.gov/awardsearch/show-award?AWD_ID=1911990</gmx:Anchor>
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http://lod.bco-dmo.org/id/dataset-parameter/852480.rdf
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http://lod.bco-dmo.org/id/dataset-parameter/852483.rdf
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http://lod.bco-dmo.org/id/dataset-parameter/852484.rdf
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&amp;lt;p&amp;gt;Dissolved Oxygen sampling and titrations from Niskin bottles follow HOT procedures. Briefly, oxygen samples were the first samples drawn from the Niskin bottles as soon as the rosette arrived on deck, free of bubbles, and fixed. Samples were analyzed with a computer controlled potentiometric titration. At 2 depths on each cast, 3 titrations were performed and had an average standard deviation of 0.4 micromol/L.&amp;lt;/p&amp;gt;

&amp;lt;p&amp;gt;Particulate Carbon and Nitrogen field and laboratory protocols follow HOT procedures (except sample analysis took place at Princeton University using a Vario ISOTOPE select EA-IRMS). Briefly, 4 to 20 L of water was collected from Niskin bottles, pre-filtered with an inline 202um mesh screen, and collected on combusted 25mm GF/F (Whatman, nominal pore size 0.7um), folded, and wrapped in clean (combusted) foil for storage at -20 degrees C until laboratory analysis. Samples were oven dried at 55-60 degrees celsius (samples were not acidified so C represents total C), pelletized in 9x11 tins, and analyzed via EA-IRMS for particulate carbon, delta-13C particulate carbon, particulate nitrogen, delta-15N particulate nitrogen. Six blank (dry) filters were analyzed for background C and N and subtracted from measured PC and PN sample values.&amp;lt;/p&amp;gt;

&amp;lt;p&amp;gt;Particulate Phosphate field and laboratory protocols follow HOT procedures. Briefly, 4 to 10 L of water was collected from Niskin bottles, pre-filtered with an inline 202um mesh screen, and collected on combusted 25mm GF/F (Whatman, nominal pore size 0.7um), folded, and placed in clean glass tube, storage at -20 degrees C until laboratory analysis. One sample from each depth was combusted in 16 x 100 mm clean glass test tubes at 450°C for 4.5 hours in a muffle furnace, allowed to cool and immersed in 10ml 0.15N HCL/vortex/ 1 hour leach/vortex/30 Minute Spin/ 1 hour color development) (5ml sample : 500ul Mixed Reagent). The liberated orthophosphate is reacted with a mixed reagent of molybdic acid, ascorbic acid and trivalent antimony to form phosphomolybdic acid. This heteropoly acid is then reduced to the colored molybdenum blue complex by ascorbic acid and the solution is measured spectrophotometrically. This procedure measures all forms of phosphorus which can be released by combustion and acid hydrolysis. Three blank (dry) filters were analyzed for background P and subtracted from measured PP sample values.&amp;lt;/p&amp;gt;</gco:CharacterString>
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		  </gmd:address>
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              <gmd:URL>http://www.bco-dmo.org</gmd:URL>
            </gmd:linkage>
          </gmd:CI_OnlineResource>
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		    <gco:CharacterString>For questions regarding this resource, please contact BCO-DMO via the email address provided.</gco:CharacterString>
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    <gmd:CI_RoleCode codeList="http://www.isotc211.org/2005/resources/Codelist/gmxCodelists.xml#CI_RoleCode" codeListValue="pointOfContact"  codeSpace="007">pointOfContact</gmd:CI_RoleCode>
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      </gmd:contact>
    </gmd:MD_MaintenanceInformation>
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    <gmi:MI_AcquisitionInformation>
    <gmi:instrument>
        <gmi:MI_Instrument>
          <gmi:identifier>
            <gmd:MD_Identifier>
              <gmd:code>
                <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/instrument/422.rdf" xlink:title="CTD Sea-Bird 911" xlink:actuate="onRequest">Sea-Bird SBE 911</gmx:Anchor>
              </gmd:code>
            </gmd:MD_Identifier>
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            <gco:CharacterString>Sea-Bird SBE 911</gco:CharacterString>
          </gmi:type>
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            <gco:CharacterString>PI Supplied Instrument Name: Sea-Bird SBE 911 PI Supplied Instrument Description:The Sea-Bird SBE 911 is a type of CTD instrument package. The SBE 911 includes the SBE 9 Underwater Unit and the SBE 11 Deck Unit (for real-time readout using conductive wire) for deployment from a vessel. The combination of the SBE 9 and SBE 11 is called a SBE 911. The SBE 9 uses Sea-Bird's standard modular temperature and conductivity sensors (SBE 3 and SBE 4). The SBE 9 CTD can be configured with auxiliary sensors to measure other parameters including dissolved oxygen, pH, turbidity, fluorescence, light (PAR), light transmission, etc.) Instrument Name: CTD Sea-Bird 911 Instrument Short Name:CTD SBE 911   Instrument Description: The Sea-Bird SBE 911 is a type of CTD instrument package.  The SBE 911 includes the SBE 9 Underwater Unit and the SBE 11 Deck Unit (for real-time readout using conductive wire) for deployment from a vessel. The combination of the SBE 9 and SBE 11 is called a SBE 911.  The SBE 9 uses Sea-Bird's standard modular temperature and conductivity sensors (SBE 3 and SBE 4). The SBE 9 CTD can be configured with auxiliary sensors to measure other parameters including dissolved oxygen, pH, turbidity, fluorescence, light (PAR), light transmission, etc.). More information from Sea-Bird Electronics. Community Standard Description: http://vocab.nerc.ac.uk/collection/L22/current/TOOL0035/</gco:CharacterString>
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            <gmd:MD_Identifier>
              <gmd:code>
                <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/instrument/469.rdf" xlink:title="Isotope-ratio Mass Spectrometer" xlink:actuate="onRequest">Vario ISOTOPE select (Elementar Isoprime)</gmx:Anchor>
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            <gco:CharacterString>Vario ISOTOPE select (Elementar Isoprime)</gco:CharacterString>
          </gmi:type>
          <gmi:description>
            <gco:CharacterString>PI Supplied Instrument Name: Vario ISOTOPE select (Elementar Isoprime) PI Supplied Instrument Description:A Vario ISOTOPE select (Elementar Isoprime) was used to quantify total C, N, and delta-13C and delta-15N. Samples are combusted/reduced at high temperature to create gases (CO2 and N2); column chromatography separates the gases; a thermal conductivity detector determines the carbon and nitrogen concentrations, followed by an isotope ratio mass spectrometer for bulk isotope composition. Measurements were calibrated with an in-house aminocaproic acid standard (ACROS) and four USGS standards (#41, #41a, #65, #25).  [C] and [N] (umol/L) were corrected for the average value measured on blank filters (n=6).  Analytical uncertainty (determined from standards with similar isotope values) was 0.2‰ for delta-15N and 0.1‰ for delta-13C.  Instrument Name: Isotope-ratio Mass Spectrometer Instrument Short Name:IR Mass Spec; IRMS   Instrument Description: The Isotope-ratio Mass Spectrometer is a particular type of mass spectrometer used to measure the relative abundance of isotopes in a given sample (e.g. VG Prism II Isotope Ratio Mass-Spectrometer). Community Standard Description: http://vocab.nerc.ac.uk/collection/L05/current/LAB16/</gco:CharacterString>
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      <gmi:instrument>
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            <gmd:MD_Identifier>
              <gmd:code>
                <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/instrument/827601.rdf" xlink:title="muffle furnace" xlink:actuate="onRequest">muffle furnace</gmx:Anchor>
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            <gco:CharacterString>muffle furnace</gco:CharacterString>
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            <gco:CharacterString>PI Supplied Instrument Name: muffle furnace PI Supplied Instrument Description:One sample from each depth was combusted in 16 x 100 mm clean glass test tubes at 450°C for 4.5 hours in a muffle furnace,  allowed to cool and immersed in 10ml 0.15N HCL/vortex/ 1 hour leach/vortex/30 Minute Spin/ 1 hour color development) (5ml sample : 500ul Mixed Reagent). Instrument Name: muffle furnace Instrument Short Name:   Instrument Description: A muffle furnace or muffle oven (sometimes retort furnace in historical usage) is a furnace in which the subject material is isolated from the fuel and all of the products of combustion, including gases and flying ash.  A type of jacketed enclosure that is used to heat a material to significantly high temperatures while keeping it contained and fully isolated from external contaminants, chemicals or substances. Muffle furnaces are usually lined with stainless steel, making them largely corrosion-resistant.</gco:CharacterString>
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      <gmi:instrument>
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            <gmd:MD_Identifier>
              <gmd:code>
                <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/instrument/413.rdf" xlink:title="Niskin bottle" xlink:actuate="onRequest">Niskin bottle</gmx:Anchor>
              </gmd:code>
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            <gco:CharacterString>Niskin bottle</gco:CharacterString>
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          <gmi:description>
            <gco:CharacterString>PI Supplied Instrument Name: Niskin bottle PI Supplied Instrument Description:Briefly, a Niskin bottle (a next generation water sampler based on the Nansen bottle) is a cylindrical, non-metallic water collection device with stoppers at both ends. The bottles were deployed in a 24 bottle rosette system mounted on a frame and combined with a CTD. Niskin bottles are used to collect discrete water samples. Instrument Name: Niskin bottle Instrument Short Name:Niskin bottle   Instrument Description: A Niskin bottle (a next generation water sampler based on the Nansen bottle) is a cylindrical, non-metallic water collection device with stoppers at both ends. The bottles can be attached individually on a hydrowire or deployed in 12, 24, or 36 bottle Rosette systems mounted on a frame and combined with a CTD. Niskin bottles are used to collect discrete water samples for a range of measurements including pigments, nutrients, plankton, etc. Community Standard Description: http://vocab.nerc.ac.uk/collection/L22/current/TOOL0412/</gco:CharacterString>
          </gmi:description>
        </gmi:MI_Instrument>
      </gmi:instrument>
      <gmi:instrument>
        <gmi:MI_Instrument>
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            <gmd:MD_Identifier>
              <gmd:code>
                <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/instrument/682.rdf" xlink:title="Titrator" xlink:actuate="onRequest">Dosimat titrator (Brinkmann)</gmx:Anchor>
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            <gco:CharacterString>Dosimat titrator (Brinkmann)</gco:CharacterString>
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            <gco:CharacterString>PI Supplied Instrument Name: Dosimat titrator (Brinkmann) PI Supplied Instrument Description:5 ml Dosimat titrator (Brinkmann) Instrument Name: Titrator Instrument Short Name:Titrator   Instrument Description: Titrators are instruments that incrementally add quantified aliquots of a reagent to a sample until the end-point of a chemical reaction is reached. Community Standard Description: http://vocab.nerc.ac.uk/collection/L05/current/LAB12/</gco:CharacterString>
          </gmi:description>
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                  <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/deployment/841636.rdf" xlink:title="Cruise" xlink:actuate="onRequest">KM1910</gmx:Anchor>
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            </gmi:identifier>
            <gmi:status>
              <gmd:MD_ProgressCode codeList="https://data.noaa.gov/resources/iso19139/schema/resources/Codelist/gmxCodelists.xml#MD_ProgressCode" codeListValue="completed"/>
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            <gmi:type>
              <gmi:MI_OperationTypeCode codeList="https://data.noaa.gov/resources/iso19139/schema/resources/Codelist/gmxCodelists.xml#MI_OperationTypeCode" codeListValue="real"/>
            </gmi:type>
            <gmi:parentOperation gco:nilReason="inapplicable"/>
            <gmi:platform>
  <gmi:MI_Platform>
    <gmi:citation>
     <gmd:CI_Citation>
       <gmd:title>
         <gmx:Anchor xlink:href="http://www.soest.hawaii.edu/UMC/KiloMoana.htm" xlink:actuate="onRequest">R/V Kilo Moana</gmx:Anchor>
       </gmd:title>
       <gmd:date gco:nilReason="unknown"/>
     </gmd:CI_Citation>
    </gmi:citation>
    <gmi:citation>
     <gmd:CI_Citation>
       <gmd:title>
         <gmx:Anchor xlink:href="http://vocab.nerc.ac.uk/collection/C17/current/33KB" xlink:actuate="onRequest">Community Standard Description</gmx:Anchor>
       </gmd:title>
       <gmd:date gco:nilReason="unknown"/>
     </gmd:CI_Citation>
    </gmi:citation>
    <gmi:identifier>
      <gmd:MD_Identifier>
        <gmd:authority>
          <gmd:CI_Citation>
            <gmd:title>
              <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/authority/1.rdf" xlink:actuate="onRequest">International Council for the Exploration of the Sea</gmx:Anchor>
            </gmd:title>
            <gmd:date gco:nilReason="unknown"/>
          </gmd:CI_Citation>
        </gmd:authority>
        <gmd:code>
          <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/platform/54009.rdf"
           xlink:title="33KB" xlink:actuate="onRequest">R/V Kilo Moana</gmx:Anchor>
        </gmd:code>
      </gmd:MD_Identifier>
    </gmi:identifier>
    <gmi:description>
      <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/platform/54009.rdf" xlink:title="R/V Kilo Moana" xlink:actuate="onRequest">vessel</gmx:Anchor>
    </gmi:description>
    <gmi:instrument gco:nilReason="unknown"/>
  </gmi:MI_Platform>
</gmi:platform>
            <gmi:plan>
              <gmi:MI_Plan>
                <gmi:status>
                  <gmd:MD_ProgressCode codeList="http://www.isotc211.org/2005/resources/Codelist/gmxCodelists.xml#MD_ProgressCode" codeListValue="completed"/>
                </gmi:status>
                <gmi:citation>
                  <gmd:CI_Citation>
                    <gmd:title>
                      <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/deployment/841636.rdf" xlink:title="Cruise" xlink:actuate="onRequest">KM1910</gmx:Anchor>
                    </gmd:title>
                    <gmd:date gco:nilReason="unknown"/>
                    <gmd:citedResponsibleParty>
                      <gmd:CI_ResponsibleParty>
                      <gmd:individualName>
                          <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/person/50675.rdf" xlink:actuate="onRequest">Matthew J. Church</gmx:Anchor>
                        </gmd:individualName>
                        <gmd:organisationName>
                          <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/affiliation/165.rdf" xlink:title="Affiliation" xlink:actuate="onRequest">University of Montana</gmx:Anchor>
                        </gmd:organisationName>
                        <gmd:contactInfo>
                        <gmd:CI_Contact>
                          <gmd:onlineResource>
                            <gmd:CI_OnlineResource>
                              <gmd:linkage>
                                <gmd:URL>https://datadocs.bco-dmo.org/docs/305/Chief_Sci_KM1910/data_docs/matt_church_EAGER_cruise_plan_06_17_2019.pdf</gmd:URL>
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                              <gmd:description>
                                <gco:CharacterString>Report describing KM1910</gco:CharacterString>
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                            </gmd:CI_OnlineResource>
                          </gmd:onlineResource>
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                      <gmd:role>
                        <gmd:CI_RoleCode codeList="http://www.isotc211.org/2005/resources/Codelist/gmxCodelists.xml#CI_RoleCode" codeListValue="principalInvestigator"/>
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                    </gmd:citedResponsibleParty>
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                </gmi:citation>
              </gmi:MI_Plan>
            </gmi:plan>
            </gmi:MI_Operation>
      </gmi:operation><gmi:platform>
  <gmi:MI_Platform>
    <gmi:citation>
     <gmd:CI_Citation>
       <gmd:title>
         <gmx:Anchor xlink:href="http://www.soest.hawaii.edu/UMC/KiloMoana.htm" xlink:actuate="onRequest">R/V Kilo Moana</gmx:Anchor>
       </gmd:title>
       <gmd:date gco:nilReason="unknown"/>
     </gmd:CI_Citation>
    </gmi:citation>
    <gmi:citation>
     <gmd:CI_Citation>
       <gmd:title>
         <gmx:Anchor xlink:href="http://vocab.nerc.ac.uk/collection/C17/current/33KB" xlink:actuate="onRequest">Community Standard Description</gmx:Anchor>
       </gmd:title>
       <gmd:date gco:nilReason="unknown"/>
     </gmd:CI_Citation>
    </gmi:citation>
    <gmi:identifier>
      <gmd:MD_Identifier>
        <gmd:authority>
          <gmd:CI_Citation>
            <gmd:title>
              <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/authority/1.rdf" xlink:actuate="onRequest">International Council for the Exploration of the Sea</gmx:Anchor>
            </gmd:title>
            <gmd:date gco:nilReason="unknown"/>
          </gmd:CI_Citation>
        </gmd:authority>
        <gmd:code>
          <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/platform/54009.rdf"
           xlink:title="33KB" xlink:actuate="onRequest">R/V Kilo Moana</gmx:Anchor>
        </gmd:code>
      </gmd:MD_Identifier>
    </gmi:identifier>
    <gmi:description>
      <gmx:Anchor xlink:href="http://lod.bco-dmo.org/id/platform/54009.rdf" xlink:title="R/V Kilo Moana" xlink:actuate="onRequest">vessel</gmx:Anchor>
    </gmi:description>
    <gmi:instrument gco:nilReason="unknown"/>
  </gmi:MI_Platform>
</gmi:platform>
          </gmi:MI_AcquisitionInformation>
  </gmi:acquisitionInformation>
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