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Samples were collected from 5 L Teflon-coated Niskin-X bottles hung on non-metal line, and clean techniques were followed throughout (Bruland et al., 1979). Niskin-X bottles were transferred to a clean lab immediately after retrieval. At most stations a single sample was collected from 20 m. Four-depth profiles extending to 200 m were collected at 6 stations along the transect.<\/p>\n
For dissolved metal analysis, 300 mL of seawater was filtered through acid-washed 47 mm 0.4 \u03bcm polycarbonate filters into 250 mL LDPE bottles which were acid-cleaned following GEOTRACES protocols (Cutter et al., 2010). A vacuum filtration apparatus was used, with all parts in contact with the sample composed of acid-washed PFA. The assembly was rinsed with 3 aliquots of sample prior to sample collection. Samples were acidified with Optima HCl to 0.024 M, double bagged, and stored for analysis on shore.<\/p>\n
Dissolved samples were analyzed using an ESI seaFAST SP2 coupled to a Perkin Elmer Nexion 350D ICP-MS. Sample aliquots were transferred to 30 mL LDPE bottles. Approximately 8 mL of sample was taken up to rinse and fill a 6 mL preconcentration loop. Samples were buffered in-line with resin-cleaned 4 M ammonium acetate buffer-adjusted to pH = 6.0 \u00b1 0.1 and passed through an ESI pre-concentration column with a 200 \u03bcL resin bed volume. The final concentration of the buffer in the samples was 0.88 M. Metals were eluted off the column with 200 \u03bcL of 1.6 M Optima-grade HNO\u2083. Eluted metals passed through a PFA nebulizer, quartz spray chamber, and nickel cones on their way to an ammonia-filled dynamic reaction cell (0.55 mL\/min flow).<\/p>\n
Quantification was achieved by standard additions automated by the seaFAST system. A standard addition solution of 6.9 nM Fe, 46 nM Mn, 4.5 nM Zn, and 1.1 nM Pb was made in 0.024 M HCl. Concentrations in this solution were quantified using an external curve. Additions were introduced as the sample filled the preconcentration loop. The volume introduced by standard additions was kept constant, with 0.024 M Optima HCl making up the difference for samples with no additions. Each sample was spiked with 2 additions averaging roughly 100% and 200% of the sample concentration.<\/p>\n
Approximately 4L of water from Niskin bottles was filtered for particulate metals. The bottles were pressurized to approximately 5 psi with 0.2 \u03bcm filtered air and seawater passed through 25 mm 0.4 \u03bcm Supor filter membranes. The membranes were housed in Swinnex polypropylene filter holders and attached to the Niskin-X bottles with Teflon tubing and polycarbonate fittings. The membrane was transferred to an acid washed petri-slide, double bagged, and kept frozen at -20\u00b0C for analysis on shore.<\/p>\n
Labile and total particulate concentrations were analyzed through sequential digestion of the Supor membranes following protocol of Rauschenberg and Twining (2015). Membranes were first leached using an acetic acid-hydroxylamine solution (Berger et al., 2008) then transferred to a PFA vial and digested with a 4M HCl\/4M HNO3\/4M HF mixture (Ohnemus et al., 2014). Reference materials and process blanks \u2013 filters that had 2 L of 0.2 \u03bcm filtered seawater passed through them \u2013were sequentially digested alongside the samples.<\/p>\n
Digests were analyzed using a Thermo Element2 HR-ICP-MS equipped with a quartz nebulizer, cyclonic spray chamber, and nickel cones. Cd was analyzed in low resolution while all other elements were analyzed in medium resolution. In-115 was used as a drift monitor, and quantification was performed using an external curve.<\/p><\/div>","@type":"rdf:HTML"}],"http:\/\/ocean-data.org\/schema\/hasBriefDescription":[{"@value":"Dissolved and particulate trace elements collected on cruise RR1604 (GO-SHIP transect IO9N) in the Eastern Indian Ocean from March to April 2016","@language":"en-US"}],"http:\/\/purl.org\/dc\/terms\/description":[{"@value":"
Dissolved and\u00a0particulate trace elements collected on cruise RR1604 (GO-SHIP transect IO9N) in the Eastern Indian Ocean from March to April 2016.<\/p><\/div>","@type":"rdf:HTML"}],"http:\/\/www.w3.org\/2000\/01\/rdf-schema#label":[{"@value":"Dissolved and Particulate Trace Elements","@type":"xsd:string"}],"http:\/\/ocean-data.org\/schema\/hasProcessingDescription":[{"@value":"
Dissolved metal samples were instrument blank corrected and quantified using standard additions. Multiple 'process blanks' (0.024 M HCl spiked with 0.1% seawater) were run daily, and daily detection limits were calculated based on 3x the standard deviation of the process blanks.<\/p>\n
All particulate ICP-MS data were normalized to an internal standard (In-115) and quantified using external calibration curves. Concentrations of each element per filter were calculated and the contribution of the process blank (measured as the elements contained in an acid-washed filter through which 0.2-\u00b5m filtered water was passed during the cruise) was then subtracted. Separate process blanks were calculated for the labile and total digestions. Element concentrations (per liter of water filtered) were calculated by dividing the per filter concentration by the volume of water passed through each filter.<\/p>\n
Data quality:\u00a0
\nData are flagged with the following:
\n1 = Good data, passed QC;
\n3 = Questionable or suspect data, used when a data point was oceanographically inconsistent;
\n4 = Bad;
\n6 = Below detection limit.<\/p>\n
BCO-DMO Processing:\u00a0modified parameter names (removed units, replaced hyphens and spaces with underscores, added \"_flag\" to flag columns, replaced blank cells with \"nd\")<\/p><\/div>","@type":"rdf:HTML"}],"http:\/\/purl.org\/dc\/terms\/identifier":[{"@value":"767658","@type":"xsd:int"}],"http:\/\/purl.org\/dc\/terms\/title":[{"@value":"Dissolved and Particulate Trace Elements"}],"http:\/\/purl.org\/dc\/terms\/date":[{"@value":"2019-05-13T15:42:54-04:00","@type":"xsd:dateTime"}],"http:\/\/purl.org\/dc\/terms\/created":[{"@value":"2019-05-13T15:42:54-04:00","@type":"xsd:dateTime"}],"http:\/\/purl.org\/dc\/terms\/modified":[{"@value":"2023-07-07T16:10:26-04:00","@type":"xsd:dateTime"}],"http:\/\/rdfs.org\/ns\/void#inDataset":[{"@id":"http:\/\/www.bco-dmo.org\/"}],"http:\/\/ocean-data.org\/schema\/namedGraph":[{"@value":"urn:bcodmo:dataset:767658","@type":"xsd:token"}],"http:\/\/ocean-data.org\/schema\/osprey_page":[{"@id":"https:\/\/www.bco-dmo.org\/dataset\/767658"}],"http:\/\/ocean-data.org\/schema\/identifier":[{"@value":"_:Identifier767658"}],"http:\/\/ocean-data.org\/schema\/datasetTitle":[{"@value":"Dissolved and particulate trace elements collected on cruise RR1604 (GO-SHIP transect IO9N) in the Eastern Indian Ocean from March to April 2016","@language":"en-US"}],"http:\/\/ocean-data.org\/schema\/abstract":[{"@value":"This dataset includes measurements of dissolved and particulate trace elements collected on cruise RR1604 (GO-SHIP transect IO9N) in the Eastern Indian Ocean from March to April 2016.","@language":"en-US"}],"http:\/\/purl.org\/dc\/terms\/rights":[{"@id":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"http:\/\/ocean-data.org\/schema\/deprecated":[{"@value":"false","@type":"xsd:boolean"}],"http:\/\/ocean-data.org\/schema\/temporalExtent":[{"@value":"_:temporalExtent767658"}],"http:\/\/ocean-data.org\/schema\/spatialCoverage":[{"@value":"_:spatialCoverage767658"}],"http:\/\/purl.org\/dc\/terms\/bibliographicCitation":[{"@value":"Twining, B., Lomas, M. 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